Abstract:The refractory gold ores containing antimony, arsenic and carbonaceous matter, and the recovery rate of gold is about 30% by whole mud cyanide,this paper studied the gold deportment of the ore, the purpose is provide the basis for the selection of the process. In the study of process mineralogy, the gravity concentration method was used to initially enrich the ore samples, and the heavy-mineral was made into polished section and scanned by using the automatic mineral analysis system BPMA. The results show that, the types of visible gold minerals in the ore include the Au-Ag series minerals and the Au-Sb series minerals, the Au-Sb series minerals has been proved to be a cyanide leaching mineral and has a little effect on gold recovery. Arsenopyrite and pyrite are the main gold-bearing minerals, the distribution rate of gold in these two minerals is 41.61% and 24.53%, respectively. Because gold is mainly inclocked in sulfide, it is advisable to use the flotation-gold concentrate pre-oxidation-cyanide recovery process to recover gold. The carbonaceous matter content in the ore is 0.12%, include graphite and amorphous carbon. In the gold recovery process, the “preg-robbing” ability of carbonaceous matter should be alert.